聚烯烃催化剂硅胶载体的制备和表征

采用并流共沉淀法制备了适用于聚烯烃催化剂的硅胶载体,为减少颗粒的聚集,在制备过程中添加一种表面活性剂。利用透射电子显微镜(TEM)、比表面积测定(BET)和X射线粉末衍射(XRD)法对制备的硅胶载体进行了表征;考察了在制备硅胶载体过程中原料硅酸钠溶液的浓度、溶液pH以及焙烧温度对产物硅胶载体的物理性能的影响。实验结果表明,硅酸钠溶液的浓度影响硅胶的初始粒子的大小,溶液pH直接影响硅酸钠的水解速率,焙烧温度影响硅胶的孔结构和比表面积。当硅酸钠溶液的浓度为0．2mol／L、溶液pH为8-9、反应温度为70℃、焙烧温度为700℃时,硅胶载体的BET比表面积为242．22m2／g、最可几孔径为16．45 nm、堆密度为0．492 1g/mL,与进口硅胶(Silica Gel 955)的物理性能相近。     

低价的市场竞争心理必须改变

概述了中国PCB产品必须走出低价的市场竞争的困境,坚决走自主创新来发展中国PCB工业的道路。     

Modeling and verification of the double frequency effect using a MEMS device

The derivation, verification, and implication of the nonlinear dynamic and frequency response of electrostatic actuator due to the double frequency effect (DFE) were reported in this study. In particular, an extra mode called half mode was observed and measured in various studies. However, a complete in-depth discussion of the effect was not reported in the past. In the present study, a second-order dynamical equation was adapted firstly to model the dynamic and frequency response of electrostatic actuator where typical harmonic input signal with a dc bias was used. Secondly, by solving the equation, complex waveform in dynamic response and an extra half mode in frequency response due to the double frequency effect can be observed and discussed. To verify the simulated result, an electrostatic driving device was fabricated using PolyMUMPS^© process. Note that in frequency response, when dc bias is equal to the amplitude of ac signal, simulated and experimental results indicated that the amplitude of half mode was one-fourth of first mode.     

以IBAC为核心处理洗浴废水的试验研究

根据洗浴废水的水质特征,采用原水→混凝沉淀-过滤→固定化生物活性炭(Immobilized Biological Activated Carbon,IBAC)→微滤膜(MF)→UV消毒→出水的工艺流程.混凝沉淀-过滤物化预处理单元可以有效地减少洗浴废水中的各类污染物.IBAC生化处理单元,实现有机污染物、LAS、浴臭等有效去除,是保证出水合格的根本措施.微滤膜发挥物理截留作用、UV消毒杀死细菌和总大肠菌群.出水水质达到＜城市供水水质标准＞(CJ/T 206-2005).     

钱塘江景观与文化关系初析

我国进入经济高速发展期后,人们在防洪抗旱得到安全保障、开发资源和治理江道等对河流的基本需求得到满足后,逐渐重视河流的景观和生态功能.从分析研究钱塘江下游河流景观特征、地理水文及人类活动对形成丰富多彩的景观的作用,以及一些以钱塘江为吟颂对象的诗词出发,初步探讨钱塘江景观多样性对人的性格、文学家风格的影响,最后从景观角度探讨河流治理的一些原则.     

中国首例缓倾铋铜金矿脉--曙光(小西南岔)铜金矿床研究新进展

据现场深入研究，结合多年生产实践，首次系统地描述了小西南岔矿床北山矿段缓倾斜铋铜金支矿脉的地质产状、规模、铜和金品位、自然铋与自然金的交生关系。在此基础上，进一步阐述了缓倾铋铜金矿脉对理论、应用研究及矿山确保铜和金入选品位的重要意义。     

3G与WLAN互连的安全协议和分析

随着无线互联网的发展,第3代移动通信系统(3G)与无线局域网(WLAN)的互连也成为研究的热点。3G系统的优势在于计费管理、漫游与安全性,WLAN系统的优势在于高带宽和低投资成本。通过3G与WLAN的互连可以实现优势互补。论文介绍了3G与WLAN互连的体系和安全结构,综述了互连的安全协议,分析了互连面临的安全挑战,并指出了现有的安全机制所存在的不足,探讨了下一步研究的方向。     

Inhibition of microbial growth in ready‐to‐eat food stored at ambient temperature by modified atmosphere packaging

This study was undertaken to develop a modified atmosphere package to control microbial growth in ready‐to‐eat (RTE) products stored at ambient temperature. Ethanol and/or limonene associated with modified atmosphere (CO₂ : O₂ : N₂ = 30% : 5% : 65%) was used to inhibit the growth of total air‐borne microorganisms and Escherichia coli in RTE products stored at 25°C. The results indicated that 0.05% ethanol vapour in the headspace was effective to inhibit the growth of air‐borne microorganisms and E. coli at 25°C for 72 h in a model study, and the effectiveness was related to ethanol content. Both 73 ppm limonene and 0.05% ethanol vapour enhanced the bacteriostatic effect of modified atmosphere in RTE sushi roll products, and no off‐flavour was detected using this formulated gas; however, no significant inhibitory effect was observed for RTE cold noodle products. This study concludes that combinations of carbon dioxide, ethanol or limonene vapours are effective to inhibit microbial growth in RTE food at ambient temperature, and the outcome may be due to the hurdle effect. Copyright © 2003 John Wiley & Sons, Ltd.     

城域网中光纤光缆的探讨

城域网的建设是今后光纤网络建设的一个热点，根据城域网的特点和系统技术要求选择光纤光缆是网络设计的重要组成部分。本根据城域网的特点和需求，对市场上现有的光纤光缆做了详细的分析和探讨，提出了城域网规划中光纤光缆选择的原则和具体的建议。